Glycosyl glycerides from the stems of ‘baekma’ cultivar of chrysanthemum morifolium

Hyun Ji Oh; Hyoung Geun Kim; Ha Seung Pak; Yun Su Baek; Oh Keun Kwon; Hak Ki Shin; Nam In Baek

doi:10.3839/jabc.2018.019

Glycosyl glycerides from the stems of ‘baekma’ cultivar of chrysanthemum morifolium

Hyun Ji Oh, Hyoung Geun Kim, Ha Seung Pak, Yun Su Baek, Oh Keun Kwon, Hak Ki Shin, Nam In Baek

Research output: Contribution to journal › Comment/debate

1 Citation (Scopus)

Abstract

The stem of Chrysanthemum morifolium, ‘Baekma’, were repeatedly extracted with 80% aqueous MeOH and the concentrates was partitioned into ethyl acetate (EtOAc), n-butyl alcohol and H₂O fraction. The repeated silica gel and octadecyl silica gel column chromatographies for the EtOAc fractions led to isolation of two glycosyl glycerides. The chemical structures of the compounds were determined as (2S)-1-O-β-D-galactopyranosyl-2,3-dilinoleoylglycerol (1) and (2S)-1-O-β-D-galactopyranosyl-2,3-dipalmitoylglycerol (2) based on spectroscopic data anlyses including nuclear magnetic resonance, mass sperctrometry, and infrared spectrometry and gas chromatography mass spectrometry.

Original language	English
Pages (from-to)	131-134
Number of pages	4
Journal	Journal of Applied Biological Chemistry
Volume	61
Issue number	2
DOIs	https://doi.org/10.3839/jabc.2018.019
Publication status	Published - 2018

Bibliographical note

Publisher Copyright:
© The Korean Society for Applied Biological Chemistry 2018.

Keywords

Baekma
Chrysanthemum morifolium
Gas chromatography mass spectrometry
Glycosyl glyceride
Nuclear magnetic resonance

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@article{154d6b8dc8ee47969a327f44c5230532,

title = "Glycosyl glycerides from the stems of {\textquoteleft}baekma{\textquoteright} cultivar of chrysanthemum morifolium",

abstract = "The stem of Chrysanthemum morifolium, {\textquoteleft}Baekma{\textquoteright}, were repeatedly extracted with 80% aqueous MeOH and the concentrates was partitioned into ethyl acetate (EtOAc), n-butyl alcohol and H2O fraction. The repeated silica gel and octadecyl silica gel column chromatographies for the EtOAc fractions led to isolation of two glycosyl glycerides. The chemical structures of the compounds were determined as (2S)-1-O-β-D-galactopyranosyl-2,3-dilinoleoylglycerol (1) and (2S)-1-O-β-D-galactopyranosyl-2,3-dipalmitoylglycerol (2) based on spectroscopic data anlyses including nuclear magnetic resonance, mass sperctrometry, and infrared spectrometry and gas chromatography mass spectrometry.",

keywords = "Baekma, Chrysanthemum morifolium, Gas chromatography mass spectrometry, Glycosyl glyceride, Nuclear magnetic resonance",

author = "Oh, {Hyun Ji} and Kim, {Hyoung Geun} and Pak, {Ha Seung} and Baek, {Yun Su} and Kwon, {Oh Keun} and Shin, {Hak Ki} and Baek, {Nam In}",

note = "Publisher Copyright: {\textcopyright} The Korean Society for Applied Biological Chemistry 2018.",

year = "2018",

doi = "10.3839/jabc.2018.019",

language = "English",

volume = "61",

pages = "131--134",

journal = "Journal of Applied Biological Chemistry",

issn = "1976-0442",

publisher = "The Korean Society for Applied Biological Chemistry",

number = "2",

}

TY - JOUR

T1 - Glycosyl glycerides from the stems of ‘baekma’ cultivar of chrysanthemum morifolium

AU - Oh, Hyun Ji

AU - Kim, Hyoung Geun

AU - Pak, Ha Seung

AU - Baek, Yun Su

AU - Kwon, Oh Keun

AU - Shin, Hak Ki

AU - Baek, Nam In

N1 - Publisher Copyright: © The Korean Society for Applied Biological Chemistry 2018.

PY - 2018

Y1 - 2018

N2 - The stem of Chrysanthemum morifolium, ‘Baekma’, were repeatedly extracted with 80% aqueous MeOH and the concentrates was partitioned into ethyl acetate (EtOAc), n-butyl alcohol and H2O fraction. The repeated silica gel and octadecyl silica gel column chromatographies for the EtOAc fractions led to isolation of two glycosyl glycerides. The chemical structures of the compounds were determined as (2S)-1-O-β-D-galactopyranosyl-2,3-dilinoleoylglycerol (1) and (2S)-1-O-β-D-galactopyranosyl-2,3-dipalmitoylglycerol (2) based on spectroscopic data anlyses including nuclear magnetic resonance, mass sperctrometry, and infrared spectrometry and gas chromatography mass spectrometry.

AB - The stem of Chrysanthemum morifolium, ‘Baekma’, were repeatedly extracted with 80% aqueous MeOH and the concentrates was partitioned into ethyl acetate (EtOAc), n-butyl alcohol and H2O fraction. The repeated silica gel and octadecyl silica gel column chromatographies for the EtOAc fractions led to isolation of two glycosyl glycerides. The chemical structures of the compounds were determined as (2S)-1-O-β-D-galactopyranosyl-2,3-dilinoleoylglycerol (1) and (2S)-1-O-β-D-galactopyranosyl-2,3-dipalmitoylglycerol (2) based on spectroscopic data anlyses including nuclear magnetic resonance, mass sperctrometry, and infrared spectrometry and gas chromatography mass spectrometry.

KW - Baekma

KW - Chrysanthemum morifolium

KW - Gas chromatography mass spectrometry

KW - Glycosyl glyceride

KW - Nuclear magnetic resonance

UR - http://www.scopus.com/inward/record.url?scp=85049219178&partnerID=8YFLogxK

U2 - 10.3839/jabc.2018.019

DO - 10.3839/jabc.2018.019

M3 - Comment/debate

AN - SCOPUS:85049219178

SN - 1976-0442

VL - 61

SP - 131

EP - 134

JO - Journal of Applied Biological Chemistry

JF - Journal of Applied Biological Chemistry

IS - 2

ER -

Glycosyl glycerides from the stems of ‘baekma’ cultivar of chrysanthemum morifolium

Abstract

Bibliographical note

Keywords

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